VIII-E-1 Spinning-Sideband Suppression in DOR NMR Spectra Using a Magic-Angle-Turning Technique

Daisuke KUWAHARA and Toshihito NAKAI

[Chem. Phys. Lett. 260, 249 (1996)]

Spinning sidebands (SSBs) in double rotation (DOR) NMR spectra for quadrupolar nuclei having half-odd-integer spins were suppressed using a two-dimensional (2D) NMR method based on a magic-angle-turning technique. The resultant 2D spectrum showed substantially no SSBs along one frequency axis whereas, along the other axis, conventional SSBs exhibited themselves.


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